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Beilstein J. Org. Chem. 2013, 9, 1487–1491, doi:10.3762/bjoc.9.169
Graphical Abstract
Figure 1: Structural formula of TEMPO (1), AZADO (2), TCNQF4 (3) and thiourea (4).
Scheme 1: Difference of the reaction products from TEMPO (1) and AZADO (2) with TCNQF4 (3).
Figure 2: Molecular structure of the adduct 5 obtained by X-ray analysis.
Scheme 2: A plausible mechanism of the reaction of AZADO (2) with TCNQF4 (3).
Figure 3: UV–vis spectra of 2 (red line), 3 (blue line) and 5 (green line).
Scheme 3: The reaction of 2 with 4 to form 6.
Figure 4: Crystal structure of the inclusion compound 6 obtained by X-ray analysis.